Aqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerization

dc.contributor.authorMorgen, Tobias O.
dc.contributor.authorLuttikhedde, Hendrik
dc.contributor.authorMecking, Stefan
dc.date.accessioned2019-07-05T12:56:45Z
dc.date.available2019-07-05T12:56:45Z
dc.date.issued2019-06-11eng
dc.description.abstractAqueous dispersions of ethylene copolymers with polar comonomers are of practical interest, e.g., as additives for paints or water-based adhesives. We report insights on the free-radical heterophase copolymerization of ethylene with vinyl acetate, acrylates, methacrylates, acrylamides, and ionic vinyl or (meth-)acrylate comonomers. Copolymers with polar comonomer contents of 0.1–10 mol % were obtained via a surfactant-free dispersion copolymerization at relatively mild conditions (250 atm, 85 °C). This allows for tuning of the low-density polyethylene particle surface properties, as demonstrated for polymer nanocomposite particles with Laponite clay in a Pickering-stabilized dispersion polymerization approach. Mechanistic insights on particle formation and stabilization are discussed.eng
dc.description.versionpublishedde
dc.identifier.doi10.1021/acs.macromol.9b00305eng
dc.identifier.urihttps://kops.uni-konstanz.de/handle/123456789/46238
dc.language.isoengeng
dc.subject.ddc540eng
dc.titleAqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerizationeng
dc.typeJOURNAL_ARTICLEde
dspace.entity.typePublication
kops.citation.bibtex
@article{Morgen2019-06-11Aqueo-46238,
  year={2019},
  doi={10.1021/acs.macromol.9b00305},
  title={Aqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerization},
  number={11},
  volume={52},
  issn={0024-9297},
  journal={Macromolecules},
  pages={4270--4277},
  author={Morgen, Tobias O. and Luttikhedde, Hendrik and Mecking, Stefan}
}
kops.citation.iso690MORGEN, Tobias O., Hendrik LUTTIKHEDDE, Stefan MECKING, 2019. Aqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerization. In: Macromolecules. 2019, 52(11), pp. 4270-4277. ISSN 0024-9297. eISSN 1520-5835. Available under: doi: 10.1021/acs.macromol.9b00305deu
kops.citation.iso690MORGEN, Tobias O., Hendrik LUTTIKHEDDE, Stefan MECKING, 2019. Aqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerization. In: Macromolecules. 2019, 52(11), pp. 4270-4277. ISSN 0024-9297. eISSN 1520-5835. Available under: doi: 10.1021/acs.macromol.9b00305eng
kops.citation.rdf
<rdf:RDF
    xmlns:dcterms="http://purl.org/dc/terms/"
    xmlns:dc="http://purl.org/dc/elements/1.1/"
    xmlns:rdf="http://www.w3.org/1999/02/22-rdf-syntax-ns#"
    xmlns:bibo="http://purl.org/ontology/bibo/"
    xmlns:dspace="http://digital-repositories.org/ontologies/dspace/0.1.0#"
    xmlns:foaf="http://xmlns.com/foaf/0.1/"
    xmlns:void="http://rdfs.org/ns/void#"
    xmlns:xsd="http://www.w3.org/2001/XMLSchema#" > 
  <rdf:Description rdf:about="https://kops.uni-konstanz.de/server/rdf/resource/123456789/46238">
    <dcterms:abstract xml:lang="eng">Aqueous dispersions of ethylene copolymers with polar comonomers are of practical interest, e.g., as additives for paints or water-based adhesives. We report insights on the free-radical heterophase copolymerization of ethylene with vinyl acetate, acrylates, methacrylates, acrylamides, and ionic vinyl or (meth-)acrylate comonomers. Copolymers with polar comonomer contents of 0.1–10 mol % were obtained via a surfactant-free dispersion copolymerization at relatively mild conditions (250 atm, 85 °C). This allows for tuning of the low-density polyethylene particle surface properties, as demonstrated for polymer nanocomposite particles with Laponite clay in a Pickering-stabilized dispersion polymerization approach. Mechanistic insights on particle formation and stabilization are discussed.</dcterms:abstract>
    <foaf:homepage rdf:resource="http://localhost:8080/"/>
    <dc:contributor>Luttikhedde, Hendrik</dc:contributor>
    <dc:creator>Morgen, Tobias O.</dc:creator>
    <dcterms:issued>2019-06-11</dcterms:issued>
    <dc:language>eng</dc:language>
    <dc:contributor>Morgen, Tobias O.</dc:contributor>
    <void:sparqlEndpoint rdf:resource="http://localhost/fuseki/dspace/sparql"/>
    <dspace:isPartOfCollection rdf:resource="https://kops.uni-konstanz.de/server/rdf/resource/123456789/29"/>
    <dc:date rdf:datatype="http://www.w3.org/2001/XMLSchema#dateTime">2019-07-05T12:56:45Z</dc:date>
    <dc:creator>Mecking, Stefan</dc:creator>
    <dcterms:isPartOf rdf:resource="https://kops.uni-konstanz.de/server/rdf/resource/123456789/29"/>
    <dc:contributor>Mecking, Stefan</dc:contributor>
    <dcterms:title>Aqueous Dispersions of Ethylene Copolymers and Their Laponite Clay Nanocomposites from Free-Radical Dispersion Polymerization</dcterms:title>
    <bibo:uri rdf:resource="https://kops.uni-konstanz.de/handle/123456789/46238"/>
    <dcterms:available rdf:datatype="http://www.w3.org/2001/XMLSchema#dateTime">2019-07-05T12:56:45Z</dcterms:available>
    <dc:creator>Luttikhedde, Hendrik</dc:creator>
  </rdf:Description>
</rdf:RDF>
kops.flag.isPeerReviewedunknowneng
kops.flag.knbibliographytrue
kops.sourcefieldMacromolecules. 2019, <b>52</b>(11), pp. 4270-4277. ISSN 0024-9297. eISSN 1520-5835. Available under: doi: 10.1021/acs.macromol.9b00305deu
kops.sourcefield.plainMacromolecules. 2019, 52(11), pp. 4270-4277. ISSN 0024-9297. eISSN 1520-5835. Available under: doi: 10.1021/acs.macromol.9b00305deu
kops.sourcefield.plainMacromolecules. 2019, 52(11), pp. 4270-4277. ISSN 0024-9297. eISSN 1520-5835. Available under: doi: 10.1021/acs.macromol.9b00305eng
relation.isAuthorOfPublication94515322-24c9-46f8-bcf7-0e7d5d28d78e
relation.isAuthorOfPublication012f23aa-a88a-4097-bd71-d96091ec9be8
relation.isAuthorOfPublication.latestForDiscovery94515322-24c9-46f8-bcf7-0e7d5d28d78e
source.bibliographicInfo.fromPage4270eng
source.bibliographicInfo.issue11eng
source.bibliographicInfo.toPage4277eng
source.bibliographicInfo.volume52eng
source.identifier.eissn1520-5835eng
source.identifier.issn0024-9297eng
source.periodicalTitleMacromoleculeseng

Dateien