Eine effiziente Synthesemethode für Diarylallenyliden(pentacarbonyl)chrom- und wolfram-Komplexe - Kristallstruktur von (CO)5Cr=C=C=CPh2
| Type of Publication: | Journal article |
| Author: | Fischer, Helmut; Reindl, David; Roth, Gerhard |
| Year of publication: | 1994 |
| Published in: | Zeitschrift für Naturforschung B ; 49b (1994). - pp. 1207-1214. - ISSN 0932-0776. - eISSN 1865-7117 |
| Title in another language: | An efficient synthesis of Diarylallenylidene Pentacarbonyl Chromium and Tungsten Complexes - Crystal Structure of (CO)5Cr=C=C=CPh2 |
| Summary in another language: |
An efficient synthesis of diarylallenylidene pentacarbonyl chromium and tungsten complexes is presented. Irradiation of M(CO)6 in THF affords (CO)5M[THF]. Substitution of the THF ligand by diarylpropargylalcoholate and subsequent desoxygenation with COCl2 gives the title compounds in good yield. The structure of diphenylallenylidene pentacarbonyl chromium has been determined by X-ray structure analysis.
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| Subject (DDC): | 540 Chemistry |
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FISCHER, Helmut, David REINDL, Gerhard ROTH, 1994. Eine effiziente Synthesemethode für Diarylallenyliden(pentacarbonyl)chrom- und wolfram-Komplexe - Kristallstruktur von (CO)5Cr=C=C=CPh2. In: Zeitschrift für Naturforschung B. 49b, pp. 1207-1214. ISSN 0932-0776. eISSN 1865-7117
@article{Fischer1994effiz-23341, title={Eine effiziente Synthesemethode für Diarylallenyliden(pentacarbonyl)chrom- und wolfram-Komplexe - Kristallstruktur von (CO)5Cr=C=C=CPh2}, year={1994}, volume={49b}, issn={0932-0776}, journal={Zeitschrift für Naturforschung B}, pages={1207--1214}, author={Fischer, Helmut and Reindl, David and Roth, Gerhard} }
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