Publikation: Synthesis of enantiopure (R,R)- and (S,S)-cis-2,3-propanoprolines
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2010
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Tetrahedron: Asymmetry. Elsevier. 2010, 21(23), pp. 2868-2871. ISSN 0957-4166. eISSN 1362-511X. Available under: doi: 10.1016/j.tetasy.2010.11.017
Zusammenfassung
A novel approach to the synthesis of an enantiopure bicyclic proline analogue, hexahydrocyclopenta[b]pyrrole-6a(1H)-carboxylic acid (‘2,3-propanoproline’), has been developed. The method relied on tandem Strecker-nucleophilic cyclization reaction of 2-(2-bromoethyl)cyclopentanone. The overall synthetic scheme included six steps and resulted in 18% overall yield of both enantiomers of the title amino acid.
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KOPYLOVA, Natalia, Oleksandr O. GRYGORENKO, Igor V. KOMAROV, Ulrich GROTH, 2010. Synthesis of enantiopure (R,R)- and (S,S)-cis-2,3-propanoprolines. In: Tetrahedron: Asymmetry. Elsevier. 2010, 21(23), pp. 2868-2871. ISSN 0957-4166. eISSN 1362-511X. Available under: doi: 10.1016/j.tetasy.2010.11.017BibTex
@article{Kopylova2010-12Synth-52038, year={2010}, doi={10.1016/j.tetasy.2010.11.017}, title={Synthesis of enantiopure (R,R)- and (S,S)-cis-2,3-propanoprolines}, number={23}, volume={21}, issn={0957-4166}, journal={Tetrahedron: Asymmetry}, pages={2868--2871}, author={Kopylova, Natalia and Grygorenko, Oleksandr O. and Komarov, Igor V. and Groth, Ulrich} }
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