Synthesis and characterisation of porous and non-porous monodisperse TiO2 and ZrO2 particles

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Widoniak_Synthesis.pdf
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2005
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Widoniak, Johanna
Eiden-Assmann, Stefanie
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Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2005, 270-271, pp. 329-334. ISSN 0927-7757. Available under: doi: 10.1016/j.colsurfa.2005.09.014
Zusammenfassung

Monodisperse spherical titania and zirconia particles of variable sizes are produced in a sol–gel synthesis from metal tetraalkoxides in alcohol with addition of a salt or a polymer solution. The influence of various precursor concentrations and the addition of different salt ions or polymer molecules on the size and on the size distribution of the final particles was investigated. The particles were characterised by electron microscopy, thermogravimetry, X-ray diffraction and electrophoresis. Nitrogen absorption measurements revealed that in the case of titania the addition of polymers yielded porous titania colloids.

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Fachgebiet (DDC)
530 Physik
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Sol - gel, Titania, Zirconia, Particles, Monodisperse
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ISO 690WIDONIAK, Johanna, Stefanie EIDEN-ASSMANN, Georg MARET, 2005. Synthesis and characterisation of porous and non-porous monodisperse TiO2 and ZrO2 particles. In: Colloids and Surfaces A: Physicochemical and Engineering Aspects. 2005, 270-271, pp. 329-334. ISSN 0927-7757. Available under: doi: 10.1016/j.colsurfa.2005.09.014
BibTex
@article{Widoniak2005Synth-17004,
  year={2005},
  doi={10.1016/j.colsurfa.2005.09.014},
  title={Synthesis and characterisation of porous and non-porous monodisperse TiO2 and ZrO2 particles},
  volume={270-271},
  issn={0927-7757},
  journal={Colloids and Surfaces A: Physicochemical and Engineering Aspects},
  pages={329--334},
  author={Widoniak, Johanna and Eiden-Assmann, Stefanie and Maret, Georg}
}
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