Qualitative analysis of waste-water from ametryne production

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1983
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Beilstein, Paul
Hütter, Ralf
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International Journal of Environmental Analytical Chemistry. 1983, 14(2), pp. 93-98. ISSN 0306-7319. eISSN 1029-0397. Available under: doi: 10.1080/03067318308071610
Zusammenfassung

s-Triazines in waste-water from the synthesis of ametryne (2-(ethylamino)4[(1-methylethyl) amino]-6-(methylthio)-l,3,5-triazine) were tentatively identified co-chromatographically by HPLC and by UV-spectra. Alkylated s-triazines (e.g. hydroxyametryne, 4-(ethylamino)-6-(methylthio)-1,3,5-triazine-2(1H)-one, and N-ethylammelide) were isolated by preparative chromatography on a reversed phase support, and were identified by mass spectrometry. Putative cyanuric acid was desalted on activated charcoal and its identity confirmed as the silylated derivative by GLC.

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570 Biowissenschaften, Biologie
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s-triazines, analysis, herbicide synthesis, by-products, biodegradation
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ISO 690COOK, Alasdair M., Paul BEILSTEIN, Ralf HÜTTER, 1983. Qualitative analysis of waste-water from ametryne production. In: International Journal of Environmental Analytical Chemistry. 1983, 14(2), pp. 93-98. ISSN 0306-7319. eISSN 1029-0397. Available under: doi: 10.1080/03067318308071610
BibTex
@article{Cook1983Quali-8032,
  year={1983},
  doi={10.1080/03067318308071610},
  title={Qualitative analysis of waste-water from ametryne production},
  number={2},
  volume={14},
  issn={0306-7319},
  journal={International Journal of Environmental Analytical Chemistry},
  pages={93--98},
  author={Cook, Alasdair M. and Beilstein, Paul and Hütter, Ralf}
}
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