Publikation: Microdomain transformations in mosaic mesocrystal thin films
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Advanced Functional Materials. 2013, 23(12), pp. 1547-1555. ISSN 1616-301X. eISSN 1099-0712. Available under: doi: 10.1002/adfm.201202294
Zusammenfassung
An easy design route via simple evaporation is reported for macroscopic mosaic thin films comprising the quaternary system of dl-lysine·HCl, poly(acrylic acid), water, and EtOH. By depositing droplets of the quaternary dispersions onto hydrophilic cover slips, the formation of macroscopic crack-free mosaic mesocrystal thin films are produced. The formation follows a multistage crystallization process, which includes the formation of a polymer-induced liquid-precursor (PILP) phase, the formation of spherulitic thin films, and the recrystallization of mosaic mesocrystal thin films. A slow cooling rate is noted to be beneficial for the mesocrystal thin films, enabling the films to be crack-free and to display low surface roughness at the nanoscale.
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JIANG, Yuan, Haofei GONG, Maciej GRZYWA, Dirk VOLKMER, Laurie GOWER, Helmut CÖLFEN, 2013. Microdomain transformations in mosaic mesocrystal thin films. In: Advanced Functional Materials. 2013, 23(12), pp. 1547-1555. ISSN 1616-301X. eISSN 1099-0712. Available under: doi: 10.1002/adfm.201202294BibTex
@article{Jiang2013Micro-26577,
year={2013},
doi={10.1002/adfm.201202294},
title={Microdomain transformations in mosaic mesocrystal thin films},
number={12},
volume={23},
issn={1616-301X},
journal={Advanced Functional Materials},
pages={1547--1555},
author={Jiang, Yuan and Gong, Haofei and Grzywa, Maciej and Volkmer, Dirk and Gower, Laurie and Cölfen, Helmut}
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<dcterms:abstract xml:lang="eng">An easy design route via simple evaporation is reported for macroscopic mosaic thin films comprising the quaternary system of dl-lysine·HCl, poly(acrylic acid), water, and EtOH. By depositing droplets of the quaternary dispersions onto hydrophilic cover slips, the formation of macroscopic crack-free mosaic mesocrystal thin films are produced. The formation follows a multistage crystallization process, which includes the formation of a polymer-induced liquid-precursor (PILP) phase, the formation of spherulitic thin films, and the recrystallization of mosaic mesocrystal thin films. A slow cooling rate is noted to be beneficial for the mesocrystal thin films, enabling the films to be crack-free and to display low surface roughness at the nanoscale.</dcterms:abstract>
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