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A W-band pulsed EPR/ENDOR study of CoIIS4 coordination in the Co[(SPPh2)(SPiPr2)N]2 complex

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2009

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Sottini, Silvia
Gast, Peter
Maganas, Dimitrios
Kyritsis, Panayotis
Groenen, Edgar J. J.

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https://doi.org/10.1039/b905726a
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Physical Chemistry, Chemical Physics (PCCP). 2009, 11(31), pp. 6727-6732. ISSN 1463-9076. eISSN 1463-9084. Available under: doi: 10.1039/b905726a

Zusammenfassung

Spin-echo detection at 95 GHz enables an electron-paramagnetic-resonance study of a cobalt complex with a bio-mimetic coordination of the transition metal by four sulfur atoms. A magnetically diluted single crystal of the complex has been investigated in great detail. Electron-nuclear double-resonance signals were observed of ligand nuclei and complete hyperfine tensors of the distinct phosphorus nuclei were derived, assigned and discussed.

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540 Chemie

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ISO 690SOTTINI, Silvia, Guinevere MATHIES, Peter GAST, Dimitrios MAGANAS, Panayotis KYRITSIS, Edgar J. J. GROENEN, 2009. A W-band pulsed EPR/ENDOR study of CoIIS4 coordination in the Co[(SPPh2)(SPiPr2)N]2 complex. In: Physical Chemistry, Chemical Physics (PCCP). 2009, 11(31), pp. 6727-6732. ISSN 1463-9076. eISSN 1463-9084. Available under: doi: 10.1039/b905726a
BibTex
@article{Sottini2009-08-21Wband-43634,
  year={2009},
  doi={10.1039/b905726a},
  title={A W-band pulsed EPR/ENDOR study of Co<sup>II</sup>S<sub>4</sub> coordination in the Co[(SPPh<sub>2</sub>)(SP<sup>i</sup>Pr<sub>2</sub>)N]<sub>2</sub> complex},
  number={31},
  volume={11},
  issn={1463-9076},
  journal={Physical Chemistry, Chemical Physics (PCCP)},
  pages={6727--6732},
  author={Sottini, Silvia and Mathies, Guinevere and Gast, Peter and Maganas, Dimitrios and Kyritsis, Panayotis and Groenen, Edgar J. J.}
}
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