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Zinc(II)-Chloride Induced Thioalkylation of Aluminium Enolates : Enantioselective Synthesis of Estradiol-3-Methyl-17-tert-Butyl Diether

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1991

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Kohler, Thomas
Taapken, Thomas

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Tetrahedron. 1991, 47(36), pp. 7583-7592. ISSN 0040-4020. Available under: doi: 10.1016/S0040-4020(01)88282-X

Zusammenfassung

Zinc(II)-chloride induced thioalkylation of the aluminium enolate 6 generated by conlugate reduction of the enone 5 leads - directly or via its trimethylsilylenol ether 6 - to alkylated hydrindanones 10 which are important intermediates in the synthesis of 19-norsteroids such as the title compound estradiol-3-methyl-17-tert-butyl diether 12

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540 Chemie

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ISO 690GROTH, Ulrich, Thomas KOHLER, Thomas TAAPKEN, 1991. Zinc(II)-Chloride Induced Thioalkylation of Aluminium Enolates : Enantioselective Synthesis of Estradiol-3-Methyl-17-tert-Butyl Diether. In: Tetrahedron. 1991, 47(36), pp. 7583-7592. ISSN 0040-4020. Available under: doi: 10.1016/S0040-4020(01)88282-X
BibTex
@article{Groth1991ZincI-9885,
  year={1991},
  doi={10.1016/S0040-4020(01)88282-X},
  title={Zinc(II)-Chloride Induced Thioalkylation of Aluminium Enolates : Enantioselective Synthesis of Estradiol-3-Methyl-17-tert-Butyl Diether},
  number={36},
  volume={47},
  issn={0040-4020},
  journal={Tetrahedron},
  pages={7583--7592},
  author={Groth, Ulrich and Kohler, Thomas and Taapken, Thomas}
}
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