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Preparation of Polystyrene-Poly(N-isopropylacrylamide) (PS-PNIPA) Core-Shell Particles by Photoemulsion Polymerization

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2006

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Lu, Yan
Ballauff, Matthias
Drechsler, Markus

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http://nbn-resolving.de/urn:nbn:de:bsz:352-202030
DOI (zitierfähiger Link)
https://doi.org/10.1002/marc.200600190
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Macromolecular Rapid Communications. 2006, 27(14), pp. 1137-1141. ISSN 1022-1336. Available under: doi: 10.1002/marc.200600190

Zusammenfassung

Monodisperse thermosensitive PS-NIPA core-shell particles composed of a PS core and a cross-linked PNIPA shell can be successfully synthesized by a novel method: photoemulsion polymerization. Cryo-TEM images indicate clearly the core-shell morphology of the PS-NIPA particles: A homogeneous regular PNIPA shell has been affixed on the spherical PS core. DLS measurements indicate that the obtained PS-NIPA latex particles are thermosensitive. The shell of PNIPA networks with different cross-linking densities can shrink and re-swell with temperature and the volume transition temperature is around 32 °C in all cases.

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Fachgebiet (DDC)
540 Chemie

Schlagwörter

core-shell particles, emulsion polymerization, latex, photopolymerization, PNIPA, thermosensitive networks

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ISO 690LU, Yan, Alexander WITTEMANN, Matthias BALLAUFF, Markus DRECHSLER, 2006. Preparation of Polystyrene-Poly(N-isopropylacrylamide) (PS-PNIPA) Core-Shell Particles by Photoemulsion Polymerization. In: Macromolecular Rapid Communications. 2006, 27(14), pp. 1137-1141. ISSN 1022-1336. Available under: doi: 10.1002/marc.200600190
BibTex
@article{Lu2006Prepa-20203,
  year={2006},
  doi={10.1002/marc.200600190},
  title={Preparation of Polystyrene-Poly(N-isopropylacrylamide) (PS-PNIPA) Core-Shell Particles by Photoemulsion Polymerization},
  number={14},
  volume={27},
  issn={1022-1336},
  journal={Macromolecular Rapid Communications},
  pages={1137--1141},
  author={Lu, Yan and Wittemann, Alexander and Ballauff, Matthias and Drechsler, Markus}
}
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