Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes
Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes
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Date
2013
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Gladkov, Eugene S.
Desenko, Sergey M.
Konovalova, Irina S.
Shishkin, Oleg V.
Vashchenko, Elena V.
Chebanov, Valentin A.
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Journal of Heterocyclic Chemistry ; 50 (2013), S1. - pp. E189-E192. - ISSN 0022-152X. - eISSN 1943-5193
Abstract
Three‐component heterocyclization of 4‐amino‐5‐carboxamido‐1,2,3‐triazole, thiopyran‐3‐one‐1,1‐dioxide, and aromatic aldehydes under ultrasonic and microwave irradiation was studied. Regardless of the reaction parameters, 5,6,7,9‐tetrahydro‐4H‐thiopyrano[3,2‐d][1,2,3]triazolo[1,5‐a]pyrimidine‐8,8‐dioxides were isolated as sole reaction products whose structures were proven with help of NMR data and X‐ray analysis.
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GLADKOV, Eugene S., Sergey M. DESENKO, Irina S. KONOVALOVA, Ulrich GROTH, Oleg V. SHISHKIN, Elena V. VASHCHENKO, Valentin A. CHEBANOV, 2013. Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes. In: Journal of Heterocyclic Chemistry. 50(S1), pp. E189-E192. ISSN 0022-152X. eISSN 1943-5193. Available under: doi: 10.1002/jhet.1503BibTex
@article{Gladkov2013-04-02Micro-42468, year={2013}, doi={10.1002/jhet.1503}, title={Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes}, number={S1}, volume={50}, issn={0022-152X}, journal={Journal of Heterocyclic Chemistry}, pages={E189--E192}, author={Gladkov, Eugene S. and Desenko, Sergey M. and Konovalova, Irina S. and Groth, Ulrich and Shishkin, Oleg V. and Vashchenko, Elena V. and Chebanov, Valentin A.} }
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