Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes

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2013
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Gladkov, Eugene S.
Desenko, Sergey M.
Konovalova, Irina S.
Shishkin, Oleg V.
Vashchenko, Elena V.
Chebanov, Valentin A.
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Journal of Heterocyclic Chemistry. 2013, 50(S1), pp. E189-E192. ISSN 0022-152X. eISSN 1943-5193. Available under: doi: 10.1002/jhet.1503
Zusammenfassung

Three‐component heterocyclization of 4‐amino‐5‐carboxamido‐1,2,3‐triazole, thiopyran‐3‐one‐1,1‐dioxide, and aromatic aldehydes under ultrasonic and microwave irradiation was studied. Regardless of the reaction parameters, 5,6,7,9‐tetrahydro‐4H‐thiopyrano[3,2‐d][1,2,3]triazolo[1,5‐a]pyrimidine‐8,8‐dioxides were isolated as sole reaction products whose structures were proven with help of NMR data and X‐ray analysis.

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ISO 690GLADKOV, Eugene S., Sergey M. DESENKO, Irina S. KONOVALOVA, Ulrich GROTH, Oleg V. SHISHKIN, Elena V. VASHCHENKO, Valentin A. CHEBANOV, 2013. Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes. In: Journal of Heterocyclic Chemistry. 2013, 50(S1), pp. E189-E192. ISSN 0022-152X. eISSN 1943-5193. Available under: doi: 10.1002/jhet.1503
BibTex
@article{Gladkov2013-04-02Micro-42468,
  year={2013},
  doi={10.1002/jhet.1503},
  title={Microwave‐Assisted and Ultrasonic‐Assisted Three‐Component Heterocyclization of 4‐Amino‐5‐carboxamido‐1,2,3‐triazole, Thiopyran‐3‐one‐1,1‐dioxide, and Aromatic Aldehydes},
  number={S1},
  volume={50},
  issn={0022-152X},
  journal={Journal of Heterocyclic Chemistry},
  pages={E189--E192},
  author={Gladkov, Eugene S. and Desenko, Sergey M. and Konovalova, Irina S. and Groth, Ulrich and Shishkin, Oleg V. and Vashchenko, Elena V. and Chebanov, Valentin A.}
}
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