A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines
A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines
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2006
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Tetrahedron Letters ; 47 (2006), 14. - pp. 2383-2385. - ISSN 0040-4039
Abstract
A safe and convenient method for the copper(II)-catalyzed diazo transfer from triflyl azide to primary amines is reported.
By replacing CH2Cl2 by toluene the formation of hazardous side products, for example, azido-chloromethane and diazidomethane can be avoided.
By replacing CH2Cl2 by toluene the formation of hazardous side products, for example, azido-chloromethane and diazidomethane can be avoided.
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540 Chemistry
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TITZ, Alexander, Zorana RADIC, Oliver SCHWARDT, Beat ERNST, 2006. A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines. In: Tetrahedron Letters. 47(14), pp. 2383-2385. ISSN 0040-4039. Available under: doi: 10.1016/j.tetlet.2006.01.157BibTex
@article{Titz2006conve-17132, year={2006}, doi={10.1016/j.tetlet.2006.01.157}, title={A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines}, number={14}, volume={47}, issn={0040-4039}, journal={Tetrahedron Letters}, pages={2383--2385}, author={Titz, Alexander and Radic, Zorana and Schwardt, Oliver and Ernst, Beat} }
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