A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines

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2006
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Radic, Zorana
Schwardt, Oliver
Ernst, Beat
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A safe and convenient method for the copper(II)-catalyzed diazo transfer from triflyl azide to primary amines is reported.
By replacing CH2Cl2 by toluene the formation of hazardous side products, for example, azido-chloromethane and diazidomethane can be avoided.

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ISO 690TITZ, Alexander, Zorana RADIC, Oliver SCHWARDT, Beat ERNST, 2006. A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines. In: Tetrahedron Letters. 2006, 47(14), pp. 2383-2385. ISSN 0040-4039. Available under: doi: 10.1016/j.tetlet.2006.01.157
BibTex
@article{Titz2006conve-17132,
  year={2006},
  doi={10.1016/j.tetlet.2006.01.157},
  title={A safe and convenient method for the preparation of triflyl azide, and its use in diazo transfer reactions to primary amines},
  number={14},
  volume={47},
  issn={0040-4039},
  journal={Tetrahedron Letters},
  pages={2383--2385},
  author={Titz, Alexander and Radic, Zorana and Schwardt, Oliver and Ernst, Beat}
}
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